http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-105153078-A
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_cc4e13141d402ceb885f368dfa042348 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D305-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D313-04 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D309-04 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D307-10 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D309-04 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D305-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D313-04 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D307-10 |
filingDate | 2015-07-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_403a887b78cd2d92ac5ed6c58881d6d8 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_65edc410d6ac61db3687e06f99893229 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_474ed41332c837400fca77c06eca4972 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_3f6734733b8f8c3e6e95fd95c1a2c4d4 |
publicationDate | 2015-12-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-105153078-A |
titleOfInvention | A kind of thioxeterocycloalkane compound and its synthesis method |
abstract | The invention belongs to the technical field of organic synthesis, and discloses a thioxeterocycloalkane compound and a synthesis method thereof. The synthesis method comprises the following steps: in a reactor, add enol, substituted or unsubstituted sodium benzene sulfinate and a solvent, add copper salt as a catalyst, stir and react at 50-150°C for 3-48 hours, after the reaction After cooling to room temperature, the solvent was distilled off under reduced pressure to obtain a crude product, which was purified by column chromatography to obtain a thioxacycloalkane compound. The synthesis method of the invention is safe and simple to operate, has low raw material prices, is easy to obtain, has good adaptability to functional groups, wide adaptability to substrates, is environmentally friendly, is beneficial to industrial production, and is widely used in the synthesis of pesticides, medicines and natural products. |
isCitedBy | http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-105481806-A |
priorityDate | 2015-07-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 24.