http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-105153078-A

Outgoing Links

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filingDate 2015-07-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_403a887b78cd2d92ac5ed6c58881d6d8
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_65edc410d6ac61db3687e06f99893229
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publicationDate 2015-12-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-105153078-A
titleOfInvention A kind of thioxeterocycloalkane compound and its synthesis method
abstract The invention belongs to the technical field of organic synthesis, and discloses a thioxeterocycloalkane compound and a synthesis method thereof. The synthesis method comprises the following steps: in a reactor, add enol, substituted or unsubstituted sodium benzene sulfinate and a solvent, add copper salt as a catalyst, stir and react at 50-150°C for 3-48 hours, after the reaction After cooling to room temperature, the solvent was distilled off under reduced pressure to obtain a crude product, which was purified by column chromatography to obtain a thioxacycloalkane compound. The synthesis method of the invention is safe and simple to operate, has low raw material prices, is easy to obtain, has good adaptability to functional groups, wide adaptability to substrates, is environmentally friendly, is beneficial to industrial production, and is widely used in the synthesis of pesticides, medicines and natural products.
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-105481806-A
priorityDate 2015-07-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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Total number of triples: 24.