http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-105004799-B
Outgoing Links
| Predicate | Object |
|---|---|
| classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N30-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N30-02 |
| filingDate | 2014-04-23-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| grantDate | 2017-07-18-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationDate | 2017-07-18-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationNumber | CN-105004799-B |
| titleOfInvention | A kind of detection method of content of 8 kinds of fixedness compositions in dragon and tiger rentan plant medicine blood plasma |
| abstract | The invention provides the method for the content of 8 kinds of fixedness compositions in a kind of utilization liquid phase tandem mass spectrum technology used in conjunction detection dragon and tiger rentan plant medicine blood plasma, this method is comprised the steps of：By mammality give the plasma containing drug after dragon and tiger rentan plant medicine after pretreatment by sample size be 1 20 μ L to Thermo Scient ific Hypersil GOLD C18 analytical column sample introductions, it is 20 DEG C 40 DEG C to control column temperature, then gradient elution was carried out according to the program of table 1 with the speed of 0.2 1.5mL/ minutes with by A phases and the mobile phase of B phase compositions, the triple level Four bar mass spectrometric hyphenated technique detection eluents of high performance liquid chromatography are utilized simultaneously, the chromatography of ions of test sample medicine and reference substance medicine is obtained, each composition and its content are detected by spectral contrast.Wherein described mobile phase A is mutually the aqueous solution of 0.01 0.02% acetic acid (containing 0.1 0.3mM ammonium acetates), and B phases are acetonitrile. |
| priorityDate | 2014-04-23-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 60.