http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-105001038-A
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_87b91e8139db80e61e82d5424f546cd4 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C23-10 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D309-08 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C17-093 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C19-075 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C22-04 |
filingDate | 2015-06-12-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_8d92d837e0d11a79f1c95e0247a7cc64 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_2b58558806b9ea744bd21b61148ad243 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_3768d997d78cdfee9f53042679fd8d24 |
publicationDate | 2015-10-28-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-105001038-A |
titleOfInvention | Novel method for synthesizing gem-dihalide compound |
abstract | The invention relates to a gem-dihalide compound. The method includes the steps that aldehyde or ketone and aroylsulfonylhydrazine are subjected to a reflux reaction in alcohol for relapse condensation dehydration, and solid hydrazone is obtained after filtration and drying are completed; afterwards, the hydrazone is reacted with N-halogeneated succinimide in solvent, and after the reaction is completed, carbonyl is obtained through column chromatography and is changed into the gem-dihalide compound. The method is high in universality, mild in condition, easy to operate and high in reaction yield. A simplest and more effective preparation approach is provided for the gem-dihalide compound. |
isCitedBy | http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-115160102-A |
priorityDate | 2015-06-12-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 82.