http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-104945348-B
Outgoing Links
Predicate | Object |
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classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07B45-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C321-28 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D217-08 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C319-24 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C323-07 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C323-09 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D239-38 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D277-78 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D263-58 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D213-76 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D275-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C313-20 |
filingDate | 2014-03-31-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2017-08-29-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2017-08-29-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-104945348-B |
titleOfInvention | Trifluoromethylthiolation reagent, synthesis method and application thereof |
abstract | The invention discloses a trifluoromethylthiolation reagent, a synthesis method and an application thereof. The present invention provides a compound 1, and also provides a preparation method of the compound 1, which comprises the following steps: reacting the compound 1a with silver trifluoromethylsulfide in an organic solvent as shown below to obtain the compound 1. The present invention also provides the application of compound 1 as a trifluoromethylthiolating reagent, which can react with amine compounds, thiol or thiophenol compounds to obtain compounds containing trifluoromethylthio. The trifluoromethylthiolation reagent 1 of the present invention has high efficiency, mild reaction conditions, high conversion rate, high yield, low production cost, wide range of applicable substrates, and is suitable for industrial production. |
priorityDate | 2014-03-31-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 143.