http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-104914180-B
Outgoing Links
Predicate | Object |
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classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N30-02 |
filingDate | 2015-05-13-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2017-03-01-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2017-03-01-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-104914180-B |
titleOfInvention | A kind of method measuring multi-form content of phytosterol in Caulis Sacchari sinensis |
abstract | The invention discloses a kind of method measuring multi-form content of phytosterol in Caulis Sacchari sinensis; plant sterol in Caulis Sacchari sinensis sample is carried out after acid hydrolysis and alkali formula saponification by the method; by ester state sterol, join saccharide sterol and acyl group is joined saccharide sterol and is converted into free state plant sterol; extract and coordinate existing plant sterol extracting method to obtain the extract containing corresponding free state sterol respectively; obtain the content of said extracted thing by high-efficient liquid phase chromatogram technology, and be calculated the content of multi-form plant sterol in Caulis Sacchari sinensis sample.The inventive method selects the soda acid combining form of ethanol solution hydrochloride and potassium hydroxide-ethanol solution, determine suitable reaction condition, select 6 ketone Dihydrocholesterols as internal standard, ether is as extractant, and coordinate the high-efficient liquid phase chromatogram condition of optimization, significantly improve extraction efficiency and the accuracy of detection. |
priorityDate | 2015-05-13-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 41.