http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-104860877-A
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_226fa86f9790e799a44846e2f6319e98 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D213-64 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D213-64 |
filingDate | 2015-06-10-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4787a53e593d43297d10603e09be084c http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_bfa19b26b0ed781f779c608877a8babb http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_1ab481d9ef51aedfd83967588d073bbe |
publicationDate | 2015-08-26-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-104860877-A |
titleOfInvention | Pyridine derivative 6-methoxy-6'-[(6-methoxypyridin-2-yl)methyl]-2,2'-pyridine and its synthesis method |
abstract | The invention discloses a pyridine derivative 6-methoxy-6'-[(6-methoxypyridin-2-yl)methyl]-2,2'-pyridine and a synthesis method thereof, the method being : Add (6'-methoxyl-[2,2'-bipyridyl]-6-yl)(6-methoxypyridin-2yl)methanone, sodium hydroxide, hydrazine hydrate (80 %), ethylene glycol, stirred at 100°C for 5 hours; added water and sodium hydroxide solution to adjust the alkalinity, and extracted the solution for two to four times; combined the organic layer, dried the organic layer, spin-dried the organic solvent, passed through a column of alumina, A yellow liquid was obtained. The present invention synthesizes an asymmetric pyridine compound, and introduces a methoxy group at the 2- and 6-positions of pyridine to facilitate the conversion between functional groups, so as to synthesize pyridine derivatives containing hydroxyl substituent groups, thereby Synthesis of metal-organic complexes with enhanced catalytic performance. |
priorityDate | 2015-06-10-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 16.