http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-104843674-B
Outgoing Links
Predicate | Object |
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classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01B32-00 |
filingDate | 2015-05-08-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2017-12-08-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2017-12-08-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-104843674-B |
titleOfInvention | The electrical heating synthetic method of more chloro polycyclic aromatic hydrocarbons |
abstract | The electrical heating synthetic method of more chloro polycyclic aromatic hydrocarbons, it is related to more chloro polycyclic aromatic hydrocarbons.Load heating source carrier in glass reactor;Load reaction solution in glass reactor;The glass reactor for installing reaction solution is put into stainless steel cavity, connects electrode, capping cavity;Mechanical pump is opened, reaction cavity is vacuumized;He gas is filled with into evacuated reaction cavity, then is vacuumized, so repeatedly 2~3 times, line replacement is entered to the residual gas of trace in cavity with He gas, the vavuum pump closed after being replaced between reaction cavity and mechanical pump;He gas is filled with into reaction unit;External electrode is connected, is turned on the power;After the completion of question response, room temperature is cooled to;Gas is introduced into reaction cavity to normal pressure;Reactant is collected, that is, obtains many more chloro polycyclic aromatic hydrocarbon products.By using tungsten filament as pyrotoxin, reacted under 5A low current, mild condition is simple to operate, and yield is considerable, and reproducibility is good. |
priorityDate | 2015-05-08-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 20.