http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-104817426-B
Outgoing Links
Predicate | Object |
---|---|
classificationCPCAdditional | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/Y02P20-584 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C25-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C17-12 |
filingDate | 2015-04-17-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2017-07-28-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2017-07-28-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-104817426-B |
titleOfInvention | A kind of preparation method of ortho-chlorotolu'ene |
abstract | The present invention relates to a kind of preparation method of ortho-chlorotolu'ene, specifically refer to using toluene as raw material, Cl 2 For chlorine source, [BMIM] Cl-nZnCl 2 (N=1,2,2.5, n are ZnCl 2 With [BMIM] Cl mol ratio)Acidic ion liquid is catalyst, and catalysis toluene prepares ortho-chlorotolu'ene;The present invention is from [BMIM] Cl-nZnCl 2 (N=1,2 or 2.5)Acidic ion liquid is used as the catalyst of chlorination, Cl 2 For chlorine source, Toluene selective chlorination reaction is carried out;This method can both improve the selectivity of ortho-chlorotolu'ene in product, again can be by [BMIM] Cl-nZnCl isolated from product 2 Ionic-liquid catalyst is reused, and production cost is reduced, beneficial to the important method of ortho-chlorotolu'ene industrialized production. |
priorityDate | 2015-04-17-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 35.