http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-104807922-B
Outgoing Links
| Predicate | Object |
|---|---|
| classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N30-02 |
| filingDate | 2015-05-26-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| grantDate | 2017-02-22-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationDate | 2017-02-22-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationNumber | CN-104807922-B |
| titleOfInvention | Detecting method for five pesticides like avemectin in crops |
| abstract | The invention discloses a detecting method for five pesticides like avemectin in crops. The detecting method at least can detect and analyze more than two of avemectin, emamectin benzoate, imidacloprid, indoxacarb and zineb. The detecting method comprises the following steps of the step 1 of preparing solution such as the solution A of 0.1% sodium hydroxide solution and the solution B of acetonitrile-water solution containing DTA-Na2 (10mmol/L) and L-cysteine (10mmol/L) and preparing the standard solution of pesticide components to be detected; the step 2 of detecting and analyzing the standard solution with UPLC-MS/MS; the step 3 of detecting samples; the step 301 of taking and smashing the samples, adding the solution A, carrying out homogenate, adding the solution B, evenly mixing in a vortex mode, ultrasonically extracting 5-20 minutes and centrifuging to take liquid supernatant; the step 302 of adding C18+GCB into the obtained liquid supernatant from the step 301, evenly mixing in a vortex mode, centrifuging to take liquid supernatant and detecting and analyzing the liquid supernatant with UPLC-MS/MS; the step 4 of processing data in the step 2 and 3 to obtain pesticide residue. The detecting method is quick, accurate, economical and practical, meets the requirements of laws and regulations and can meet the requirements of daily detection. |
| priorityDate | 2015-05-26-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 85.