http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-104744706-B
Outgoing Links
Predicate | Object |
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classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08G77-60 |
filingDate | 2015-04-22-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2017-07-21-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2017-07-21-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-104744706-B |
titleOfInvention | The synthetic method of high ceramic yield Polycarbosilane |
abstract | The invention discloses a kind of synthetic method of high ceramic yield Polycarbosilane, molecular weight is pressed 100 in 500 1500 Polycarbosilane and allyl compound:(12~4) after mixing; it is dissolved in dimethylbenzene; it is placed in reaction vessel, adds organolithium reagent, heats up and reacted under protective gas protection; it is 100~150 DEG C to control maximum temperature; and insulation reaction 2~8 hours, after reaction terminates, it is filtered to remove insoluble matter; solvent is evaporated off, high ceramic yield Polycarbosilane is obtained.The present invention has that reaction condition is easily controllable, method is easy, and product has self-crosslinking ability, and the characteristics of Si H and adjustable allyl content, can conveniently prepare liquid or the high ceramic yield Polycarbosilane of solid-state. |
priorityDate | 2015-04-22-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 39.