http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-104725265-A
Outgoing Links
| Predicate | Object |
|---|---|
| assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_082b80fb6b52c4109b8c0204d8a64e26 |
| classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C233-13 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C233-66 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C231-02 |
| filingDate | 2015-04-13-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_ef8ff4c9c68059d1393397234f05ffb7 |
| publicationDate | 2015-06-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationNumber | CN-104725265-A |
| titleOfInvention | A kind of synthetic method of nitroamide compound |
| abstract | The present invention provides a synthetic method of nitroamide compounds shown in the following formula (III), The method comprises: in an organic solvent, in the presence of a palladium catalyst and a base, the compound of the following formula (II), the compound of the formula (III) and nitromethane are reacted to obtain the compound of (I), Wherein, R 1 is H, C 1 -C 6 alkyl, C 1 -C 6 alkoxy or halogen; R 2 is C 1 -C 6 alkyl, phenyl or benzyl; X is halogen. Through the selection of catalyst, alkali and organic solvent, the method has synergistic effects and effects, and has achieved good yield, so that the method has good application in the field of organic synthesis, especially in the technical field of pharmaceutical intermediate synthesis. The application prospect and industrialization potential can fully meet the extensive needs of the fields of medicine and chemical industry. |
| priorityDate | 2015-04-13-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 17.