http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-104710632-B
Outgoing Links
| Predicate | Object |
|---|---|
| classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/A61K41-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B82Y30-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B82Y40-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01G3-12 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08K3-30 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/A61P35-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01G29-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08L71-08 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08J3-12 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/A61K47-04 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08K7-24 |
| filingDate | 2014-09-23-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| grantDate | 2017-04-05-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationDate | 2017-04-05-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationNumber | CN-104710632-B |
| titleOfInvention | A kind of Cu of Pegylation3BiS3The preparation method of hollow nano-sphere |
| abstract | The invention discloses a kind of Cu of Pegylation 3 BiS 3 The preparation method of hollow nano-sphere, comprises the steps：1）Prepare A mixed solutions：By copper chloride CuCl 2 , five water bismuth nitrate Bi (NO 3 ) 3 5H2O, is dissolved in ethylene glycol, and stirring obtained A mixed solutions, CuCl after 1 hour 2 、Bi(NO 3 ) 3 5H2O, the ratio of ethylene glycol are 0.45 mmol:0.15 mmol:55 ml;Prepare B mixed solutions：By L cysteine, PEG（Mn=2000）, ethylene glycol is dissolved in, stirring obtained B mixed solutions after 1 hour；L cysteine, PEG, the ratio of ethylene glycol are 0.6 mmol：4 mL:5 mL；CuCl 2 、Bi(NO 3 ) 3 •5H 2 The mol ratio of O and L cysteine is 3:1:4；2）By step 1）The A mixed solutions for obtaining 1 h of oil bath back flow reaction under the conditions of 200 DEG C, obtains A reactant liquors；By step 1）In the B mixed solutions injection A reactant liquors for obtaining, stirring was transferred in autoclave after 1 hour, and 1 h is reacted under the conditions of 200 DEG C, was cooled down, centrifugation, and washing is dried, obtains final product the Cu of Pegylation 3 BiS 3 Hollow nano-sphere. |
| priorityDate | 2014-09-23-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 35.