http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-104591986-A
Outgoing Links
| Predicate | Object |
|---|---|
| assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_2425e03c2ac444c7ef5d68bb10d611cf |
| classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C45-36 |
| classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C47-228 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C45-36 |
| filingDate | 2015-01-26-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_5e02ce20e4d053f348fc03291f7aad29 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_58d78965d8d7ceae4cabb20ef94be268 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_e22b5e0074d0f7c69868c1b30a705575 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_9f708416c2baaec50724dab82ddd11a7 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_c0963e0f46b154fddbeb81f030bf2011 |
| publicationDate | 2015-05-06-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationNumber | CN-104591986-A |
| titleOfInvention | A kind of method preparing solanaldehyde |
| abstract | The invention provides a kind of method for preparing solanum aldehyde, first weigh a-methylstyrene, organic solvent, catalyst and pro-oxidant, the quality of described a-methylstyrene, organic solvent, catalyst and pro-oxidant Ratio is 1:2.5～12:0.01～0.3:1～4, described catalyst is metal phthalocyanine catalyst, and described prooxidant is aldehydes; and pro-oxidants are added into a reaction container, excess oxygen is fed into the container, and magnetic stirring is carried out at 5-45° C. for 2-10 hours to obtain solanaldehyde. The method of the present invention avoids the step-by-step treatment operations such as isomerization, reduction, salt formation, and hydrolysis reported in the prior art, and the intermediates of each step can be easily prepared from solanum aldehyde without separation process, realizing the realization of solanum nigrum "One-pot" production of aldehydes. The method of the invention is simple to operate, saves energy and is easy to be industrialized. |
| priorityDate | 2015-01-26-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 23.