http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-104557792-B

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Predicate Object
classificationCPCAdditional http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/Y02P20-584
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D301-12
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D303-32
filingDate 2015-01-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2016-11-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2016-11-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-104557792-B
titleOfInvention A kind of production method of alpha, beta-lonone epoxide
abstract The invention discloses the production method of a kind of β ionoionone epoxide in production of flavor field; it is under nitrogen protection; control temperature 0-40 DEG C of reaction system, with two (3,5 two trifluoromethyl) diselenide for catalyst; in a solvent; with hydrogen peroxide as oxidant, oxidation of beta ionoionone, it is thus achieved that epoxidation product 4 [2; 2,6 trimethyl 7 bases in oxabicyclo [4.1.0] heptan 1] 3 butylene 2 ketone.This method energy highly selective synthesis 4 [2,2,6 trimethyl 7 base in oxabicyclo [4.1.0] heptan 1] 3 butylene 2 ketone;Used oxidant cleans, and economy is high, and after oxidant reduction, by-product is only water, to environment non-hazardous;This method does not use metallic catalyst, and the organic selenium catalyst used is to ecological friendly;Reaction is carried out in temperate condition, neutral environment, little to equipment corrosion, durable, and catalyst can recycle, thus is more suitable for commercial production.
priorityDate 2015-01-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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