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filingDate 2015-01-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2016-05-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2016-05-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-104557485-B
titleOfInvention The application of miniflow field reactor in Friedel-Crafts reaction
abstract The invention discloses the application of miniflow field reactor in Friedel-Crafts reaction, by nano oxidized iron particles filled in immobilization micro passage reaction, for the Friedel-Crafts acylation reaction of catalysis aromatic hydrocarbon and chloroacetic chloride. Wherein, described nano-sized iron oxide particle prepares as follows: the inorganic matter of iron content distilled water is dissolved, again the aqueous solution of the aqueous solution of inorganic base and iron content inorganic matter is pumped into respectively in microchannel module reaction unit simultaneously, keep time of staying 30s-1min, under room temperature, react, product is centrifugal, and precipitation is through washing, dry, then in Muffle furnace 500 DEG C of roasting 2h. The present invention reacts the nano oxidized iron particles filled of preparation for catalysis aromatic hydrocarbon in immobilization micro passage reaction with the Friedel-Crafts of chloroacetic chloride, feed stock conversion is up to 100%.
priorityDate 2015-01-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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