http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-104497308-B
Outgoing Links
Predicate | Object |
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classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08G73-02 |
filingDate | 2014-12-11-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2017-07-04-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2017-07-04-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-104497308-B |
titleOfInvention | A kind of preparation method of poly- adjacent mercaptoaniline nanofiber |
abstract | The invention provides a kind of preparation method of poly- adjacent mercaptoaniline nanofiber.Its preparation method is:By N diphenyl-para-phenylene diamines with adjacent mercaptoaniline in molar ratio for 0.05 0.2 are placed in reaction vessel, and acidic aqueous solution is added by adjacent mercaptoaniline concentration dilution to 0.01 0.1 mol/L, temperature control is at 0 35 DEG C, during aqueous oxidizing agent solution disposably to add to the reaction system again, react 8 20 hours, be then centrifuged for, wash and obtain.It is an advantage of the invention that:The addition of N diphenyl-para-phenylene diamine small molecules can induce the generation of poly- neighbour's mercaptoaniline nanofibrous structures;Changing N diphenyl-para-phenylene diamines little molecular concentration can regulate and control the pattern for gathering adjacent mercaptoaniline nanofiber;Synthetic method is simple, and reappearance is high, and product quality is preferable. |
priorityDate | 2014-12-11-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 21.