http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-104497235-B
Outgoing Links
Predicate | Object |
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classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08F222-38 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C09K11-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08F220-54 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08F292-00 |
filingDate | 2014-12-14-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2017-02-01-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2017-02-01-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-104497235-B |
titleOfInvention | Temperature responsive fluorescent carbon nanoparticle hybrid microgel and preparation method thereof |
abstract | The invention relates to a temperature responsive fluorescent carbon nanoparticle hybrid microgel and a preparation method thereof. The method comprises the following steps: (1) weighing a proper amount of fluorescent carbon nanoparticles, preparing a fluorescent carbon nanoparticle solution by using dichloromethane, adding an acyl chloride monomer, reacting for 10 hours at room temperature, removing a reaction solvent, adding and spin-drying; (2) weighing the obtained double-bond fluorescent carbon nanoparticles and dispersing and dissolving in the fluorescent carbon nanoparticles; and transferring into a reaction container, introducing nitrogen to discharge air, adding a crosslinking agent, sodium dodecyl sulfate and refined N-isopropylacrylamide and stirring; introducing nitrogen, heating, and when the reaction liquid flows back, weighing an initiator and adding the initiator into a three-necked flask; (3) continuously introducing nitrogen and stirring; carrying out reflux react for 5-16 hours at 50-90 DEG C, and then stopping reaction; and (4) cooling to room temperature, filtering, and taking the filtrate and carrying out dialysis for 48 hours. The product prepared by the method is non-toxic, has a very good temperature response by fluorescence and has a good application prospect in drug controlled release, temperature sensing and the like. |
priorityDate | 2014-12-14-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 45.