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filingDate 2014-11-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2016-08-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2016-08-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-104478679-B
titleOfInvention The preparation technology of γ, δ-higher unsaturated ketone and method of purification
abstract The invention discloses a kind of γ, the preparation technology of δ higher unsaturated ketone, including addition unsaturated alcohol with organo aluminum catalyst, addition Acetacetic acid alkyl ester, react and reduce pressure distilation steps, under 0.06~0.0Mpa pressure condition, organo-aluminium is selected to make catalyst, the selectivity of reaction is more than 99.5%, and conversion ratio is more than 98%, and corresponding product yield is more than 95%.The purified technique of product of preparation, final products purity is more than 99.5%, and the rate of recovery is more than 99%, and heel rate is less than 0.5%.
priorityDate 2014-11-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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