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filingDate 2014-12-15-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2016-08-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2016-08-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-104475011-B
titleOfInvention A kind of remove the preparation method of the magnetic mesoporous silica adsorbent of aflatoxin in edible oil
abstract A kind of remove the preparation method of the magnetic mesoporous silica adsorbent of aflatoxin in edible oil, specifically comprise the following steps that (1) dissolves rice hull ash and alkali solid obtains rice hull ash aqueous slkali;(2) it is rapidly added strong aqua ammonia, heated and stirred after adding iron salt;Precipitation filters and separates, washing, is dried, grinds;(3) take magnetic particle and cationic surfactant is placed in beaker, drip adjuvant, ultrasonic disperse, stirring, add rice hull ash aqueous slkali, regulate pH value, maintain temperature to continue stirring;(4) being aged after reaction, centrifugation precipitates, and deionized water wash for several times, is calcined after precipitation drying, carbonization, removed cationic surfactant, and product is magnetic mesoporous silica adsorbent.Preparation technology of the present invention is simple, mild condition, low raw-material cost, and gained magnetic mesoporous silica adsorbent specific surface area is high, can effectively remove aflatoxin B in edible oil 1 , and be prone to separate with food material, it is possible to recycling.
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