http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-104447885-A
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_80ed4a2280d90214f21515d153b17802 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/H01F1-42 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F19-00 |
filingDate | 2013-09-22-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_7dc7802843cdf3e3c4ba31aaee2cac88 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_3be770af65ac1a34306a60631fb36cd0 |
publicationDate | 2015-03-25-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-104447885-A |
titleOfInvention | Furan ring-containing paramagnetic carborane derivative and preparation method thereof |
abstract | The invention relates to a furan ring-containing paramagnetic carborane derivative and a preparation method thereof. The molecular formula of the furan ring-containing paramagnetic carborane derivative is shown as follows: C19H24B10O2S2Co, and the molecular weight of the furan ring-containing paramagnetic carborane derivative is 515.57. A synthetic method of the compound comprises the following steps: with dichloromethane as a solvent, simultaneously adding CpCoS2C2B10H12 and furan alkynyl ketone in 20-35mL of dichloromethane according to the mass ratio of 1 to 1.5, carrying out reaction at the temperature of 15-25 DEG C for 12-17h, pumping the solvent by virtue of decompression, separating and purifying a residual solid crude product by virtue of a column chromatography method, and eluting the residual solid crude product by virtue of a mixed solvent of petroleum ether and dichloromethane to obtain a pure yellow solid compound. |
isCitedBy | http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-110105404-A |
priorityDate | 2013-09-22-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 21.