http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-104341459-A
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_d281e953d189bcfe2507ba7faba72c25 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07F17-02 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F17-02 |
filingDate | 2014-09-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4899178c48dda4e6577b7ad5ea375702 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_1234faa33d63caa6eddab589b297aa01 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_6f36bece7d2a2b22129ffac6596e467c http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_98f8219c1f299f75c83d932489a33cd7 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_70fa5a6ed2b82089f35b958050c284d3 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_aff58bb953e6ad7dffe4b69e94a4beb1 |
publicationDate | 2015-02-11-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-104341459-A |
titleOfInvention | N-(4-ferrocenylphenyl)amide compounds, and synthesis method thereof application thereof |
abstract | The invention provides N-(4-ferrocenylphenyl)amide compounds, and a synthesis method thereof application thereof. The technical scheme is as follows: the structure of is disclosed as general formula (I). The synthesis method comprises the following steps: 1) dissolving 4-ferrocenylaniline in anhydrous pyridine to obtain a 4-ferrocenylaniline pyridine solution, and cooling for later use; 2) dissolving aromatic acyl chloride in anhydrous pyridine, pouring into a round-bottom flask, stirring and cooling to 0-5 DEG C; 3) dropwisely adding the cooled 4-ferrocenylaniline pyridine solution into the solution obtained in the step 2), reacting for 4-9 hours, and carrying out vacuum filtration; 4) pouring the filtrate into water to deposit abundant precipitate, and carrying out vacuum filtration to obtain a solid; and 5) recrystallizing the solid with a solvent, and purifying by chromatography to obtain the target product. The method is simple and convenient, and has the advantages of high operability, high yield and high universality. |
isCitedBy | http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-112920228-A |
priorityDate | 2014-09-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 53.