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filingDate 2014-09-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4899178c48dda4e6577b7ad5ea375702
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publicationDate 2015-02-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-104341459-A
titleOfInvention N-(4-ferrocenylphenyl)amide compounds, and synthesis method thereof application thereof
abstract The invention provides N-(4-ferrocenylphenyl)amide compounds, and a synthesis method thereof application thereof. The technical scheme is as follows: the structure of is disclosed as general formula (I). The synthesis method comprises the following steps: 1) dissolving 4-ferrocenylaniline in anhydrous pyridine to obtain a 4-ferrocenylaniline pyridine solution, and cooling for later use; 2) dissolving aromatic acyl chloride in anhydrous pyridine, pouring into a round-bottom flask, stirring and cooling to 0-5 DEG C; 3) dropwisely adding the cooled 4-ferrocenylaniline pyridine solution into the solution obtained in the step 2), reacting for 4-9 hours, and carrying out vacuum filtration; 4) pouring the filtrate into water to deposit abundant precipitate, and carrying out vacuum filtration to obtain a solid; and 5) recrystallizing the solid with a solvent, and purifying by chromatography to obtain the target product. The method is simple and convenient, and has the advantages of high operability, high yield and high universality.
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-112920228-A
priorityDate 2014-09-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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