http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-104311531-A

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filingDate 2014-10-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 2015-01-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-104311531-A
titleOfInvention A kind of 2,5-dinaphthyl oxane derivative and preparation method thereof
abstract The invention discloses a 2,5-dinaphthyloxane derivative, which is characterized in that the structural formula of the derivative is as follows: , where R=R`orR≠R`, R, R` are hydrogen atoms, ethyl or propylalkyl groups, which are 4-substituted-1-naphthylcarbaldehyde and 2-(4-substituted)naphthyl -1,3-Propanediol, in the ratio of 1mol:0.8~2.0mol, dissolved in organic solvents such as DMF or toluene, catalyzed by silicon-based solid acid catalyst, reacted under ultrasonic radiation at 40~150℃ for 0.5~2.0h , to obtain 2,5-dinaphthyloxane derivatives. The invention has the characteristics of high fluorescence quantum efficiency, unfavorable crystallization and simple preparation method.
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