http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-104198623-B
Outgoing Links
| Predicate | Object |
|---|---|
| classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N30-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N30-02 |
| filingDate | 2014-09-26-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| grantDate | 2015-12-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationDate | 2015-12-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationNumber | CN-104198623-B |
| titleOfInvention | Detect the method that in porcine tissue, menbutone is residual |
| abstract | The invention discloses and detect the method that in porcine tissue, menbutone is residual, first the porcine tissue after intramuscular injection menbutone parenteral solution is taken, homogenate after chopping, homogenised tissue acetonitrile extracts, and is rotary evaporated to dryness under the vacuum of 60 DEG C after extract is centrifugal in temperature, cold really after, mobile phase ultrasonic dissolution is added in residue, then centrifugal, collect supernatant, the supernatant filtering with microporous membrane of 0.22 μm, filtrate is need testing solution; Secondly accurately weighed menbutone reference substance, making concentration with mobile phase dilution after dissolving with acetonitrile is 10 ± 1 μ g/mL, obtained reference substance solution; Finally need testing solution and reference substance solution are adopted high performance liquid chromatography inspection, record chromatogram, by external standard method with calculated by peak area, obtains the residual quantity of menbutone in tissue; The method specificity is good, highly sensitive, reproducible, can detect the residual of menbutone in porcine tissue fast, for the residual quantity controlling menbutone in animal food provides reliable method. |
| priorityDate | 2014-09-26-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 61.