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filingDate 2014-07-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2017-01-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2017-01-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-104091931-B
titleOfInvention Multi-edge MoS2 nano piece/graphene composite nanomaterial and preparation method thereof
abstract The invention discloses a multi-edge MoS2 nano piece/graphene composite nanomaterial and a preparation method thereof, wherein the multi-edge MoS2 nano piece/graphene composite nanomaterial is formed by compounding few layers of multi-edge MoS2 nano pieces and graphene; the ratio of the amount of substance of MoS2 to the graphene is (1:1)-(1:4); the preparation method comprises the steps of firstly, carrying out ultrasonic dispersion on graphene oxide into deionized water, feeding ionic liquid, and fully stirring; sequentially feeding L-cysteine and sodium molybdate, fully mixing for fully dissolving to obtain a mixed disperse system, transferring the mixed disperse system into a hydrothermal reaction kettle, and carrying out hydrothermal reaction for 24 hours at the temperature of 230-250 DEG C; and naturally cooling to the room temperature to obtain a solid hydrothermal product, carrying out centrifugal collection on the solid hydrothermal product, washing, drying, and carrying out heat treatment to obtain the multi-edge MoS2 nano piece/graphene composite nanomaterial. The method has the characteristics of being simple and convenient, and has the advantage of being easy to expand in industrialized application. The prepared composite nanomaterial is wide in application range.
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