http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-104072655-B
Outgoing Links
Predicate | Object |
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classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08F212-08 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08F230-08 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08F220-28 |
filingDate | 2014-06-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2017-01-04-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2017-01-04-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-104072655-B |
titleOfInvention | Fructus Rubi shape single dispersing hydridization submicron microsphere and preparation method thereof |
abstract | The present invention provides the preparation method of a kind of Fructus Rubi shape single dispersing hydridization submicron microsphere, including: according to St:HEMA:MPS: initiator: the mass ratio of water is 1.8:0~0.2:0~0.2:0.04~0.08:40 obtains raw material St, HEMA, MPS, initiator, water;Water in raw material is added to the reaction vessel of protective atmosphere filling, and is heated to 60~90 DEG C;Adding monomer St, HEMA and MPS and initiator in reaction vessel, wherein the MPS joining day is monomer St, HEMA and between initiator adds first 8 hours and add latter 4 hours to described monomer St, HEMA and initiator;And carry out polyreaction 1~12 hours.In the above-mentioned preparation method of the present invention, by adjusting rate of charge and the prehydrolysis time of MPS, thus the Fructus Rubi shape colloidal particle of surface particle size, surface roughness is prepared in control;The Fructus Rubi shape single dispersing hydridization submicron microsphere particle surface simultaneously generated has hydroxyl and silicone hydroxyl, is beneficial to be combined with inorganic nano-particle, promotes nanometer particle load and the application function of catalysis, and need not other auxiliary reagent. |
priorityDate | 2014-06-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 34.