http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-104072409-B

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classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D213-82
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D213-81
filingDate 2014-06-27-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2016-08-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2016-08-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-104072409-B
titleOfInvention A kind of synthetic method of pyridine amides
abstract The invention discloses the synthetic method of a kind of pyridine amides, described method is: the pyridine cyanides shown in Formula II is raw material, with water as solvent, under the effect of catalyst ETS 10 molecular sieve, it is heated to 100 150 DEG C react, to reaction completely, reactant liquor post processing prepares pyridine amides shown in formula I to TLC tracing detection.The present invention, with ETS 10 molecular sieve as catalyst, carries out the hydrolysis of pyridine cyanogen, obtains single picolinamide class product, conversion ratio 100%, yield more than 95%, and catalyst can reuse more than 5 times.
priorityDate 2014-06-27-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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