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publicationDate 2014-09-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-104030965-A
titleOfInvention Method for preparing lenticin monomer from vaccaria segetalis
abstract The invention relates to a method for separating lenticin monomer from a traditional Chinese medicinal material vaccaria segetalis, and belongs to the field of traditional Chinese medicines. The preparation technology comprises: degreasing vaccaria segetalis seeds, and performing ethanol refluxing extraction; performing extraction by successively using dichloromethane, ethyl acetate and water-saturated n-butanol; performing preparative thin-layer chromatography; and separating by using preparative high performance liquid chromatography, performing reduced-pressure condensation, and drying. The chemical structure of the lenticin monomer is determined by employing physical and chemical property discriminating technology, infrared spectroscopy, ultraviolet spectroscopy, mass spectroscopy and nuclear magnetic resonance technology. The method is simple, rapid, less in need solvent and relatively high in yield, and has relatively high economic value and academic value.
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