http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103940654-B
Outgoing Links
Predicate | Object |
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classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N1-28 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N30-90 |
filingDate | 2014-05-06-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2016-08-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2016-08-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-103940654-B |
titleOfInvention | Method and the thin-layer chromatography detection method of vitamin E is extracted from useless white bole |
abstract | The invention discloses a kind of method extracting vitamin E from fats and oils processing gives up white bole, take the useless white bole after using in grease processing technique, add the ethanol solution of 95%, ultrasonic extraction 3 times;Merge upper solution, centrifugal, solvent is evaporated off, adds n-hexane, reflux extraction, stratification, take upper strata n-hexane layer, n-hexane is evaporated off and i.e. obtains vitamin E.Present invention also offers the thin-layer chromatography scanning detection method of a kind of vitamin E: (1) thin-layer chromatography: by sample liquid, and vitamin E oil titer point is on same High Performance Thin silica gel plate, pre-equilibration 20 minutes, plate is put into expansion cylinder, ascending development, taking-up is dried, and again launches, taking-up is dried, and red fuming nitric acid (RFNA) develops the color;(2) thin layer scanning, detection is calculated the regression equation of the relation of vitamin E standard solution quality and integrating peak areas value, then calculates the mass concentration of vitamin E in sample liquid.There is the advantages such as simple, quick, accurate, reliable, stable. |
priorityDate | 2014-05-06-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 24.