http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103936587-A

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filingDate 2014-03-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 2014-07-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-103936587-A
titleOfInvention Triacetin preparation method
abstract The invention relates to a triacetin preparation method, which comprises that: glycerol and acetyl chloride respectively pass through a graphite tubular reactor, the tubular reactor is cooled by using salt water, a material enters a vapor-liquid separator from the tubular reactor to separate most of hydrogen chloride gas, and then enters a thermal insulation reaction kettle so as to be subjected to a thermal insulation reaction, reduced pressure evaporation is performed to remove the produced hydrogen chloride gas, and a falling film absorber is adopted to absorb the produced hydrochloric acid by-product. The preparation method has characteristics of no requirement of catalyst and water-carrying agent, clean production achieving, low cost, simple process, high product purity, high reaction efficiency and low energy source consumption.
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-115677497-A
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type http://data.epo.org/linked-data/def/patent/Publication

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