http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103915528-B
Outgoing Links
Predicate | Object |
---|---|
classificationCPCAdditional | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/Y02P70-50 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/H01L31-0324 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/H01L31-1832 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/H01L31-18 |
filingDate | 2014-03-28-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2017-06-13-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2017-06-13-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-103915528-B |
titleOfInvention | A kind of synthetic method of copper-zinc-tin-sulfur copper sulfide copper and tin sulphur film |
abstract | The invention discloses a kind of synthetic method of copper-zinc-tin-sulfur copper sulfide copper and tin sulphur film, comprise the following steps:(1)Prepare electrolyte:Mantoquita, zinc salt, pink salt, sodium thiosulfate, trisodium citrate and tartaric acid are dissolved into water respectively, are then remixed, pH value is adjusted after being well mixed;(2)Cleaning substrate:Metal Mo pieces wipe surface as substrate with sodium hydroxide solution, remove surface rusty stain, are then gradually cleaned by ultrasonic in ethanol, deionized water, remove surface oil stain;(3)Electrochemical deposition:Cleaned substrate is put into the electrolyte for having prepared, setting deposition voltage and the time and is started, deposition takes out substrate after terminating, with substantial amounts of deionized water and alcohol flushing and dried up;(4)By step(3)The sample for obtaining is calcined 1 hour in nitrogen or argon gas, obtains copper-zinc-tin-sulfur copper sulfide copper and tin sulphur film.The method low cost, process is simple, and obtained properties of sample is excellent. |
priorityDate | 2014-03-28-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 51.