http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103910594-B
Outgoing Links
Predicate | Object |
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classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C5-29 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C13-615 |
filingDate | 2014-04-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2016-04-20-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2016-04-20-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-103910594-B |
titleOfInvention | A kind of preparation method of 1,3-dimethyladamantane |
abstract | The present invention relates to chemical field, especially 1, the preparation method of 3-dimethyladamantane, the step of this preparation method is: A, with perhydro acenaphthene for raw material, add the aluminum trichloride (anhydrous) as catalyzer, continue to drip a small amount of water at 80-100 DEG C of temperature, carry out rearrangement reaction and produce to obtain 1,3-dimethyladamantane reaction solution; B, removal aluminum trichloride catalyst, obtain 1,3-dimethyladamantane crude product; C, rectifying tower rectifying on 1, the 3-dimethyladamantane crude product of step B is obtained 1,3-dimethyladamantane finished product.The method is simple to operate, clean environment firendly, yield are high, equipment investment is few. |
priorityDate | 2014-04-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 30.