http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103896840-B
Outgoing Links
Predicate | Object |
---|---|
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01C1-242 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D223-10 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D201-04 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01C1-242 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D201-04 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D223-10 |
filingDate | 2012-12-28-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2018-06-05-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2018-06-05-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-103896840-B |
titleOfInvention | The method and apparatus of continuous production epsilon-caprolactams |
abstract | The present invention provides a kind of method of continuous production ε caprolactams, this method contains in order, a) by i) oleum and/or sulfuric acid and ii) cyclohexanone oxime is input to Beckmann rearrangement area;B) mixture of the caprolactam containing ε of generation is discharged from Beckmann rearrangement area;C) ammonia is added to the mixture of the caprolactam containing ε;D) ammonium sulfate is isolated from the mixture of the caprolactam containing ε;E) ε caprolactams are extracted from the mixture of the caprolactam containing ε in organic solvent;F) add water conservancy and from the ε caprolactams of extraction remove organic solvent in distillation zone with distilling;It is characterized in that the reaction heat that at least part of Beckmann rearrangement area generates exchanging to distillation zone.The present invention also provides the ε caprolactams suitable for implementing the equipment of the above method and being obtained according to the above method. |
priorityDate | 2012-12-28-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 42.