http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103884802-B
Outgoing Links
| Predicate | Object |
|---|---|
| classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N30-56 |
| filingDate | 2012-12-19-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| grantDate | 2016-03-02-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationDate | 2016-03-02-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationNumber | CN-103884802-B |
| titleOfInvention | A kind of memory loss shellfish poison molecular engram integral column and application thereof |
| abstract | The present invention relates to a kind of preparation method and application of memory loss property shellfish poison molecular engram integral column.By the template molecule of suitable proportioning, function monomer, crosslinking chemical, pore-foaming agent (lauryl alcohol, 1,4-butylene glycol) be dissolved in dimethyl sulfoxide (DMSO), ultrasonic mixing 5 minutes, leave standstill 20 minutes, add initiating agent (azoisobutyronitrile) and account for 0.5 ~ 1% of monomer total amount, fill nitrogen deoxygenation 5 minutes, this solution is full of quartz capillary, end-blocking, 60 ~ 70 DEG C of constant temperature are polymerized 12 ~ 14 hours, kapillary is connected on high performance liquid chromatography infusion pump, cleaning removing template molecule and pore-foaming agent, finally obtain the capillary monolithic column with good separation effect.Molecular engram integral column prepared by the present invention has good selective recognition and little resistance to mass tranfer, as high performance liquid chromatography microtrabeculae, can realize the separation to domoic acid in shellfish samples, enrichment and detection. |
| priorityDate | 2012-12-19-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 41.