http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103818938-B
Outgoing Links
Predicate | Object |
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classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01F7-30 |
filingDate | 2014-02-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2016-05-04-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2016-05-04-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-103818938-B |
titleOfInvention | A kind of preparation method of high thermal stability modified aluminium oxide supports |
abstract | The invention discloses a kind of method of preparing high thermal stability modified aluminium oxide supports, be characterized in using the aluminium ingot of purity >=99.5% and the lanthanide rare metal of purity >=99% according to mass fraction 10:1~200:1, in frequency induction melting furnace, melting obtains Al-La alloy cast ingot in a vacuum, ingot casting makes by pressure processing the strip that thickness is 0.05~0.5mm, cut into 1~50mm long, under the condition that the rectangle strip that 1~50mm is wide and isopropyl alcohol are catalyst at 1~5% aluminum trichloride (anhydrous), 85 ~ 95 DEG C of back flow reaction are after 4 ~ 8 hours, prepare aluminium isopropoxide and isopropyl alcohol group of the lanthanides metal dibasic alkoxide, this dibasic alkoxide is 60 ~ 80 DEG C of not exclusively hydrolysis, be decompressed to after 0.09~0.01MPa at 60 ~ 85 DEG C, through distillation, hydrolysate is 85 ~ 95 DEG C of oven dry, 800~900 DEG C of calcinings, finally prepare the metal-modified high thermal stability aluminum oxide carrier of lanthanide rare powder body material. |
priorityDate | 2014-02-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 31.