http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103789801-B
Outgoing Links
Predicate | Object |
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classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C25D3-38 |
filingDate | 2014-01-13-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2017-03-15-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2017-03-15-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-103789801-B |
titleOfInvention | A kind of non-cyanide pre-plating copper plating solution and preparation method thereof |
abstract | The present invention relates to a kind of non-cyanide pre-plating copper plating solution and preparation method thereof, the electroplate liquid is comprised the following components in percentage by weight:Chelating agent 1~60%, mantoquita 0.5~30%, balance of water, the formula of the chelating agent is M x H y P n O 3n+1 R z , wherein M is any one or more in alkali metal ion and NH4+, and R is acyl group, and the formula of mantoquita is Cu x/2 H y P n O 3n+1 R z , x, n and z be positive integer, and y is 0 or positive integer, x+y+z=n+2.Preparation method is as follows:(1)The preparation of chelating agent:By the hybrid reaction in molar ratio of the acid salt containing the alkali of M, carbonate or bicarbonate and phosphoric acid, the unitary organic acid containing R bases or multicomponent organic acid, then reactant liquor 0.5~10h of one-step polymerization acquisitions chelating agent finished product under the conditions of 100~800 DEG C;(2)The preparation of mantoquita:Chelating agent is mixed homogeneously in aqueous phase system in molar ratio with cupric compound, reacts 0.5~1h in 25~100 DEG C, reaction terminate after through centrifugation and dry mantoquita;(3)The preparation of electroplate liquid:Each component is mixed in proportion, electroplate liquid is obtained. |
priorityDate | 2014-01-13-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 65.