Predicate |
Object |
assignee |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_70fbe08b7c540157200696115221f654 |
classificationCPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D307-77 |
classificationIPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D307-93 |
filingDate |
2012-11-02-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate |
2015-06-03-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_2f8ae1e02b5cf415562ae2ea7755dcc4 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_ee087cf49592987b7175b03c9ee4fe4c http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_276967a6e5e6a8a6da6ec36f413add82 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_38192c425a2e968fb8f15174157dc244 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b508152cce0f8cf76b37f2a12db8aa7f http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_bd939439533fa800b672b8695b94b986 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_44b9a1de1d075df4572a608b7d07ba95 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_93a762171a9dd5ff16bfa1d7e0c332cb http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4e16be5b7256ad154e3a529d002c4253 |
publicationDate |
2015-06-03-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber |
CN-103788037-B |
titleOfInvention |
Method for purifying carabrone |
abstract |
The invention discloses a method for purifying carabrone. The method comprises the following steps: (1) soaking or ultrasonically extracting carpesium abrotanoides in a water solution of inorganic strong base at 0-100 DEG C; then, filtering, adjusting the pH value of filter liquor to be 1-7 by the inorganic strong base to generate deposits; (2) removing the deposits generated in the step (1), and then extracting supernatant liquid by an organic solvent to obtain extracting liquid; and (3) performing silica column chromatography on the extracting liquid obtained from the step (2) to obtain the carabrone. The method is easy to operate; the obtained carabrone is relatively high in purity. |
priorityDate |
2012-11-02-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type |
http://data.epo.org/linked-data/def/patent/Publication |