http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103755980-B

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Predicate Object
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08F8-30
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08F220-60
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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08F220-56
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08F283-06
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08J3-07
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filingDate 2014-01-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2015-12-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2015-12-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-103755980-B
titleOfInvention A kind of preparation method of autofluorescence nano-micelle
abstract A preparation method for autofluorescence nano-micelle, relates to the preparation method of organic fluorescence materials.Add in tetrahydrofuran solution by hydrophilic monomer 1, hydrophilic monomer 2 and initiator, degassed through continuous freeze thawing, after applying argon gas protection, polymerization, the more sudden cold stopped reaction of liquid nitrogen, select normal hexane as precipitation agent, obtains random copolymers after repeatedly purifying; The molecule and random copolymers that contain color development functional group are dissolved in methylene dichloride, add anhydrous slufuric acid reactive magnesium, remove magnesium sulfate by suction filtration, select normal hexane as precipitation agent purifying; Random copolymers containing color development modified with functional group is dissolved in tetrahydrofuran (THF), is then added to the water, leave standstill volatilization tetrahydrofuran (THF), obtain autofluorescence nano-micelle.Adopt one-step synthesis method random copolymers, and graft on random copolymers by containing chromophoric molecule with the form of dynamic key, method is simple, and be easy to control, reaction conditions is gentle, without the need to adding metal catalyst, and the easy purifying of product.
priorityDate 2014-01-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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