http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103739490-B
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_d4d7206ead88c846616742e8c39de673 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C67-48 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C69-732 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C67-48 |
filingDate | 2013-12-31-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2015-03-25-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_5cc49460aadc942daca85ceeb18e0bc7 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_57af20ea3cb75934280ae46f36ee658e |
publicationDate | 2015-03-25-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-103739490-B |
titleOfInvention | Method for extracting and purifying chlorogenic acid from smilax or congeneric plants thereof |
abstract | The invention discloses a method for extracting and purifying chlorogenic acid from the roots or leaves of smilax or congeneric plants thereof. The method comprises the following steps: grinding the roots, stalks or leaves of the smilax or the congeneric plants thereof; performing sieving through a 2# sieve; performing ultrasonic or reflux extraction through water or low-concentration ethanol, performing filtration, and recovering a solvent until alcohol smell disappears; performing filtration, and loading a filtered solution to polystyrene type macroporous adsorption resin; performing gradient elution; extracting eluate through ethyl acetate, recovering ethyl acetate, and separating out a chlorogenic acid crystal; re-crystallizing 50 percent of ethanol water solution for 3-4 times. The purity of chlorogenic acid obtained through the method can be greater than 98.0 percent. According to the method, the smilax is used as a raw material for extracting chlorogenic acid for the first time, so that medicinal components of the smilax are fully utilized; the method is simple in process, short in production period and high in product purity, and has a broad application value and good social and economic benefits. |
priorityDate | 2013-12-31-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 38.