http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103739490-B

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classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C67-48
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C69-732
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C67-48
filingDate 2013-12-31-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2015-03-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_5cc49460aadc942daca85ceeb18e0bc7
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_57af20ea3cb75934280ae46f36ee658e
publicationDate 2015-03-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-103739490-B
titleOfInvention Method for extracting and purifying chlorogenic acid from smilax or congeneric plants thereof
abstract The invention discloses a method for extracting and purifying chlorogenic acid from the roots or leaves of smilax or congeneric plants thereof. The method comprises the following steps: grinding the roots, stalks or leaves of the smilax or the congeneric plants thereof; performing sieving through a 2# sieve; performing ultrasonic or reflux extraction through water or low-concentration ethanol, performing filtration, and recovering a solvent until alcohol smell disappears; performing filtration, and loading a filtered solution to polystyrene type macroporous adsorption resin; performing gradient elution; extracting eluate through ethyl acetate, recovering ethyl acetate, and separating out a chlorogenic acid crystal; re-crystallizing 50 percent of ethanol water solution for 3-4 times. The purity of chlorogenic acid obtained through the method can be greater than 98.0 percent. According to the method, the smilax is used as a raw material for extracting chlorogenic acid for the first time, so that medicinal components of the smilax are fully utilized; the method is simple in process, short in production period and high in product purity, and has a broad application value and good social and economic benefits.
priorityDate 2013-12-31-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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