http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103664634-B
Outgoing Links
Predicate | Object |
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classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C209-08 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01J23-72 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C211-11 |
filingDate | 2012-09-06-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2017-06-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2017-06-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-103664634-B |
titleOfInvention | For loaded catalyst prepared by 1,2 propane diamine |
abstract | The invention discloses a class loaded catalyst, 1,2 propane diamine are prepared with this catalyst, its central synthetic steps is as follows:Add 1,2 dichloropropanes, ammoniacal liquor, loaded catalyst, reactor at the uniform velocity to be rotated in homogeneous reactor in a kettle., aminating reaction is carried out at 140 DEG C~170 DEG C of reaction temperature and prepares 1,2 propane diamine, the yield of product is higher than 65%.After reaction terminates, unreacted ammonia is removed first, then air-distillation obtains the aqueous solution of 1,2 propane diamine.Advantages of the present invention:(1) loaded catalyst catalysis prepares 1,2 propane diamine, obtains yield higher;(2) it is raw material using the dichloropropane of accessory substance 1,2 produced during production chloropropene, production cost greatly reduces;(3) course of reaction is simple, easy to operate;(4) this method safety and environmental protection, beneficial to industrialized production. |
priorityDate | 2012-09-06-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 26.