http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103642024-B
Outgoing Links
Predicate | Object |
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classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08G63-85 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08G18-42 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08G65-28 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08G18-48 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08G63-672 |
filingDate | 2013-10-23-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2016-01-13-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2016-01-13-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-103642024-B |
titleOfInvention | A kind of preparation method of terephthalic acid polyester polyether polyol |
abstract | The invention discloses a kind of preparation method of terephthalic acid polyester polyether polyol, comprise the following steps: 1) will reclaim in alcohol, terephthalic acid, organotin disposable input pet reaction still; Pass into N2, slowly heat up, insulation; Vacuumize, treat product acid number≤1.5mg? stopped reaction during KOH/g; Cooling press leaches material, obtains terephthalic acid kind polyester polyvalent alcohol.2) above-mentioned intermediate product and multi-metal cyanide, the vitriol oil are dropped in polyether reactant still, decompression; Drop into the mixture of propylene oxide, oxyethane to reactor, slowly heat up, reaction 0.5 ~ 1h, continue to heat up, and be incubated 0.5 ~ 3h; Treat that Pressure Drop is to below-0.04MPa, vacuumizes, pressure and temperature maintain respectively-0.095 ~-0.090MPa, 105 ~ 110 DEG C; Cooling press leaches material, obtains terephthalic acid polyester polyether polyol. |
priorityDate | 2013-10-23-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 32.