http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103603050-B
Outgoing Links
Predicate | Object |
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classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C30B29-62 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C30B7-14 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C30B29-16 |
filingDate | 2013-11-13-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2016-02-03-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2016-02-03-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-103603050-B |
titleOfInvention | A kind of method of liquid phase making ZnO nano whisker |
abstract | The invention discloses a kind of method of liquid phase making ZnO nano whisker.Take zinc solution as raw material, under low temperature 2 ~ 8 DEG C of conditions, add sodium hydroxide solution, control mixing solutions zinc alkali mol ratio in (1:6) ~ (1:7) scope, obtain containing Zn (OH)n 4 2- the solution of ion presoma, add micro-surfactant sodium dodecyl base benzene sulfonic acid sodium salt again, the first mild stirring 1 ~ 2h at ambient temperature of the mixing solutions obtained, then constant temperature ageing 5 ~ 6h in the water-bath of 75 ~ 90 DEG C, products therefrom after filtration, washing, then through weak ammonia washing, dry, obtain size uniform, there is good crystallinity, diameter 80 ~ 100nm, length 4 ~ 5 μm, length-to-diameter ratio is about the ZnO nano whisker of 50.The present invention is the preparation of pure liquid phase, has the advantages such as raw material is easy to get, technique is simple, the reaction times is short, reaction conditions is gentle, green non-pollution. |
priorityDate | 2013-11-13-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 29.