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assignee http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_d6a6f422b091ba12ea61d4adbf1b0e8e
classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D249-06
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D249-06
filingDate 2013-09-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2015-04-01-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_d64c94b01f3d983c0609a5c3e4c25a78
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_46a2de7cca142b87964bfa587dc6ecc7
publicationDate 2015-04-01-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-103483279-B
titleOfInvention Preparation method of 1,4-disubstituted triazole compound
abstract The invention discloses a preparation method of a 1,4-disubstituted triazole compound. The preparation method comprises the following steps of adding a bivalent copper salt, neopentanoic acid, aromatic amine and substituted acetophenone p-toluenesulfonylhydrazone into an organic solvent, heating the resulting solution to 100-110 DEG C for reaction, and carrying out posttreatment to obtain the 1,4-disubstituted triazole compound after the reaction is finished. The preparation method is simple in steps; the raw materials are easily available; the reaction does not need to be carried out in an anhydrous anaerobic condition; more importantly, the trinitride which is toxic and easy to explode does not need to be used; and therefore the preparation method is convenient to operate.
priorityDate 2013-09-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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Total number of triples: 46.