http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103467255-B
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_f7332f833c19a9d550ba29618764ff99 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C41-26 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C43-23 |
filingDate | 2013-09-13-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2015-07-01-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_6c35e0156b64c7b693b9deb73c6aadd5 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_faafc56e55c21d9dd4df98797d79f8c9 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_83c585f856c990803650f28a6ef4add3 |
publicationDate | 2015-07-01-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-103467255-B |
titleOfInvention | Synthetic method of natural product pterostilbene |
abstract | The invention provides a synthetic method of natural product pterostilbene, and is mainly used for solving the problems of high cost, low yield and non-adaptability for large-scale industrial production of the existing pterostilbene preparing method. The synthetic method of pterostilbene comprises the following steps of: 1) preparing an intermediate toluylene; 2) preparing 3,5-dialkyl-4-O-tetrahydropyrane toluylene; 3) preparing the pterostilbene. According to the invention, as HBr is adopted for a bromination reaction, the preparation of 3,5-dimethoxybenzylbromide is mild in reaction conditions, simple in aftertreatment and low in cost, and the yield is above 90%; the whole process is simple to operate, easy in obtaining of raw materials, and applicable for industrial production. |
priorityDate | 2013-09-13-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 85.