http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103467255-B

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assignee http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_f7332f833c19a9d550ba29618764ff99
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C41-26
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C43-23
filingDate 2013-09-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2015-07-01-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_6c35e0156b64c7b693b9deb73c6aadd5
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_faafc56e55c21d9dd4df98797d79f8c9
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_83c585f856c990803650f28a6ef4add3
publicationDate 2015-07-01-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-103467255-B
titleOfInvention Synthetic method of natural product pterostilbene
abstract The invention provides a synthetic method of natural product pterostilbene, and is mainly used for solving the problems of high cost, low yield and non-adaptability for large-scale industrial production of the existing pterostilbene preparing method. The synthetic method of pterostilbene comprises the following steps of: 1) preparing an intermediate toluylene; 2) preparing 3,5-dialkyl-4-O-tetrahydropyrane toluylene; 3) preparing the pterostilbene. According to the invention, as HBr is adopted for a bromination reaction, the preparation of 3,5-dimethoxybenzylbromide is mild in reaction conditions, simple in aftertreatment and low in cost, and the yield is above 90%; the whole process is simple to operate, easy in obtaining of raw materials, and applicable for industrial production.
priorityDate 2013-09-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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