http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103466684-B

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assignee http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_653c418e41edbb4e1ce8bc5e53e70cec
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C25B1-26
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01G5-02
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01J27-10
filingDate 2013-09-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2015-03-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_a61f5cc995551ff8ea523a53084fce31
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_af19ef1d183c806cd47f0b022bbbc178
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publicationDate 2015-03-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-103466684-B
titleOfInvention High-activity cubic-block silver chloride micron-crystal and electrochemical preparation method thereof
abstract The invention relates to a high-activity cubic-block silver chloride micron-crystal and an electrochemical preparation method thereof. The high-activity cubic-block silver chloride micron-crystal is of pure cubic-phase silver chloride and has a {100}-face-exposed crystal face structure. The method comprises the steps of adding sodium sulfate into a certain volume of deionized water, stirring to dissolve solids, then, adding sodium chloride, and stirring for mixing uniformly; transferring the prepared mixed solution into an H-shaped electrochemical reaction tank, adding a silver sheet to one end of the reaction tank, connecting the end of the reaction tank to the positive pole of a constant-potential power supply, adding a platinum sheet to the other end of the reaction tank, and connecting the other end of the reaction tank to the negative pole of the constant-potential power supply; regulating the voltage output by the power supply, oxidizing the silver sheet so as to generate silver ions, reacting for 30-40 minutes at room temperature, filtering and washing precipitates at the bottom of the reaction tank nearby the silver sheet electrode, and drying in a thermostat, thereby obtaining the cubic-block silver chloride micron-crystal. Under visible light, the activity of a photocatalyst formed by the cubic-block silver chloride micron-crystal is relatively high.
priorityDate 2013-09-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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