http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103450034-B
Outgoing Links
| Predicate | Object |
|---|---|
| assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_d42d445a771ee30222eddbe900c23c70 |
| classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C215-28 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C213-08 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C205-16 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C201-12 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01J31-22 |
| filingDate | 2013-09-22-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| grantDate | 2014-11-19-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_054e6b39ad977cafd84758244cf1bcb3 |
| publicationDate | 2014-11-19-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationNumber | CN-103450034-B |
| titleOfInvention | Chiral nickel complex |
| abstract | Provided is a chiral nickel complex. According to the chemical formula of the chiral nickel complex, the synthetic method of the chiral nickel complex comprises the steps of weighing 2.2630g (0.015mol) of L-phenylalaninol and 1.2442g (0.005mol) of hexahydrate nickel chloride, adding the L-phenylalaninol and the hexahydrate nickel chloride to a 100ml round-bottom flask, adding about 45ml of absolute ethyl alcohol as solvents, carrying out heating and stirring backflow for 48 hours, carrying out filtering in heating, spinning filter liquid to be dry, changing the solvents to be prepared into saturated solutions, carrying out standing and self volatilization, and treating filter residues in the same way. After a period of time, a crystal suitable for being used for an X-single crystal diffraction test is separated out, and is fully washed for 3-4 times with petroleum ether, vacuum drying is carried out for 30min, a pure target product is obtained, and the complex shows certain catalytic performance in the Henry reaction of benzaldehyde. |
| priorityDate | 2013-09-22-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 33.