http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103435493-B
Outgoing Links
Predicate | Object |
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classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C201-08 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C205-50 |
filingDate | 2013-09-10-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2016-01-20-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2016-01-20-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-103435493-B |
titleOfInvention | The preparation method of a kind of nitro-oleic acid and derivative thereof |
abstract | The invention discloses a kind of method preparing nitro-oleic acid and derivative thereof, belong to organic synthesis field.Present method with oleic acid or Witconol 2301 for raw material, pass into nitrogen-containing oxide (NO) gas wherein and oxygen mix one-step synthesis goes out nitro-oleic acid or nitro-oleic acid methyl esters, synthesis yield is at 10-25%, and the purity of the finished product obtained with TLC separation is further higher than 90%.The method is simple, and yield is high, does not use mercury chloride (HgCl in prior synthesizing methodn 2 ), the chemical reagent of the severe toxicity such as phenyl Selenium monobromide, be one be eco-friendly preparation in macroscopic quantity method.The present invention not only can for promote and development nitrofatty acid and the research of derivative thereof provide experiment and theoretical foundation, also will expand its application in field of biology further. |
priorityDate | 2013-09-10-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 56.