http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103406135-B

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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C02F1-30
filingDate 2013-08-07-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2014-12-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_ba21399e49771ab6eabdab3f7a2ce47f
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publicationDate 2014-12-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-103406135-B
titleOfInvention Preparation method for synthesizing N-TiO2@WSe2 photocatalyst through sol-gel method and application of N-TiO2@WSe2 photocatalyst
abstract The invention belongs to the technical field of environmental-friendly inorganic nano materials and relates to a preparation method for synthesizing a N-TiO2@WSe2 photocatalyst through a sol-gel method and application of the N-TiO2@WSe2 photocatalyst. The preparation method comprises the following steps: preparing a titanium ethanol solution; dropwise adding a thiocarbamide ethanol solution; adding WSe2 and stirring uniformly; dropwise adding acidic ethanol water to obtain sol; aging, calcining at high temperature and grinding to obtain the N-TiO2@WSe2 photocatalyst. In the N-TiO2@WSe2 photocatalyst prepared by the method, N-TiO2 particles of about 50 nm are uniformly distributed on the surface of WSe2, so that the N-TiO2@WSe2 photocatalyst can be used for photodegradation of wastewater containing antibiotics. The dispersity of N-TiO2 is improved, the photocatalytic activity of N-TiO2@WSe2 is enhanced, and tetracycline degradation validates that the photocatalytic activity is 69.7% higher than that of unadulterated TiO2. The preparation method is simple, low in cost and high in controllability, the yield of products is high and environmental protection is achieved.
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