http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103364515-B
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_b564e3ce0542c9d4e7813f6b3d2e4f19 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N30-88 |
filingDate | 2013-07-03-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2014-12-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_ab061b6e593a38430114d949de79e891 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_2dcab49030d564cbc26759a443daa749 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_ed08a8710c8e003d15678f1497592c4a http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_80bc97a169003bc4f4845e7f5059ec8f http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_2488acb3d1534b74109d9cc489da99e4 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_0e63fd529a132a5adbf5ce32558f4388 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_032231d95d89e95e5e1cf3ce33226a41 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_3d49931391672673c99f195770fcf84c http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_a2f2b217aeada925f8833f6a6b497fe2 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4741a9616a8b7e07da78ac53fca160bd |
publicationDate | 2014-12-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-103364515-B |
titleOfInvention | Method for detecting aldehydes in rice |
abstract | The invention discloses a method for detecting aldehydes in rice. According to the method, the method is realized by employing a headspace derived solid phase micro-extraction-gas chromatography-mass spectrometry method. The method comprises the following steps of: grinding a rice sample, adding the detected sample into a headspace bottle, introducing protective gas, inserting an extraction head into the headspace bottle filled with derivative liquid for deriving for 20 minutes, and inserting the extraction head into a headspace sample introduction bottle, wherein the extraction temperature is 40 DEG C, and the extraction time is 80 minutes; detecting in a gas chromatograph-mass spectrometer. The fineness and headspace derivatization conditions of the ground rice particles are optimized, so that newly generated aldehydes in the analysis process are avoided, and the accuracy of an experimental result is improved. According to the detection method, five steps of adsorbing derivative liquid of the extraction head, deriving and extracting the aldehydes, performing sample introduction, separating and measuring can be sequentially finished in a process, automation is realized, the operation is simple, the detection efficiency and accuracy are improved, and absolute quantification of nine aldehydes in rice is realized. |
priorityDate | 2013-07-03-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 53.