http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103304481-B
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_4d99d60815ba9a3be5836ad83198b52d |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C277-08 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C275-54 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D233-38 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C279-28 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/D06L4-12 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/D06L4-13 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C273-18 |
filingDate | 2012-03-15-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2015-07-01-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_3e2490f18e85658ed6dacfd3c825848d http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_a47c7d4eb924ae521cce617ae7d450af http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_44b274dc741711193072188adf02c345 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_2cc12ae5a92309d1e728997dd5b5adc3 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_67c239d2cb62673e0b8c6697c218fe44 |
publicationDate | 2015-07-01-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-103304481-B |
titleOfInvention | Preparation method of low-temperature oxygen bleaching activator as well as scouring and bleaching formula and method thereof |
abstract | The invention discloses a preparation method of a low-temperature oxygen bleaching activator. The method comprises the two steps of synthesizing an intermidate and generating the low-temperature oxygen bleaching activator: 1) adding a diamine compound, an organic amine neutralizer and a solvent A into a four-opening flask; heating until realizing solvent A reflux; 2) dissolving 4-dimethylamino benzoyl chloride with the solvent A; adding into the four-opening flask; preserving heat and refluxing for 5 to 6 hours; 3) cooling and separating out a precipitate; performing suction filtration, washing and drying on the precipitate, thereby obtaining the intermidate; 4) adding the intermidate and a solvent B into the four-opening flask; slowly dripping dimethyl sulfate for 1 to 2 hours; continuously stirring for 1 to 2 hours after dripping; 5) removing the solvent in a steaming manner, thereby obtaining the low-temperature oxygen bleaching activator. When the low-temperature oxygen bleaching activator is used for structuring a hydrogen peroxide and activator scouring and bleaching system, the whiteness of a fabric can reach the level of conventional bleaching; the handfeel of the fabric is superior to that obtained by the conventional bleaching. Thus, the damage to the fabric is reduced; the energy consumption is decreased; the production efficiency is improved. |
priorityDate | 2012-03-15-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 60.