http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103303881-B
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_d4d43054b27c1bdcd8a9ef729f5c4328 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01B25-047 |
filingDate | 2013-06-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2015-07-15-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_56a07c8f518b81a75e25ebf150f2f065 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_0f3e77e4a898f43f8088c1e5c79d25df http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_db12fb1a420456b53953229c41d98240 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_bcaebd97b7652ab5337f2ed6f85e1c98 |
publicationDate | 2015-07-15-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-103303881-B |
titleOfInvention | Yellow phosphorus water-phase oxidizing dearsenification and water-phase oxidant recycling method |
abstract | The invention discloses a yellow phosphorus water-phase oxidizing dearsenification and water-phase oxidant recycling method. Peracetic acid of which the concentration is 10-50% is taken as a water-phase oxidant; the yellow phosphorus is put into the water-phase oxidant to fully agitate and mix; the mass ratio of the water-phase oxidant to the yellow phosphorus is (1:1)-(10:1); the reaction temperature in the water-phase oxidant is controlled at 50-85 DEG C; the reaction time is controlled between 2 hours and 4 hours; the temperature of an arsenic water phase is controlled at 100-125 DEG C to carry out boiling deoxygenation; the time is controlled at 10-30 minutes; phosphorus pentasulfide or sulfuretted hydrogen is added to the deoxidized arsenic water phase to carry out dearsenification treatment; adding phosphorus pentoxide and hydrogen peroxide to react after filtering and exposing filtrate; the dearsenified water phase is prepared into peracetic acid; the peracetic acid is recycled in a new batch of dearsenification of arsenic yellow phosphorus after the concentration is adjusted. The method has the advantages of being convenient to operate, low in production cost, environment-friendly and safe; the water-phase oxidant can be recycled. |
priorityDate | 2013-06-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 52.