http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-103303881-B

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assignee http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_d4d43054b27c1bdcd8a9ef729f5c4328
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01B25-047
filingDate 2013-06-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2015-07-15-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_56a07c8f518b81a75e25ebf150f2f065
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_0f3e77e4a898f43f8088c1e5c79d25df
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_db12fb1a420456b53953229c41d98240
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publicationDate 2015-07-15-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-103303881-B
titleOfInvention Yellow phosphorus water-phase oxidizing dearsenification and water-phase oxidant recycling method
abstract The invention discloses a yellow phosphorus water-phase oxidizing dearsenification and water-phase oxidant recycling method. Peracetic acid of which the concentration is 10-50% is taken as a water-phase oxidant; the yellow phosphorus is put into the water-phase oxidant to fully agitate and mix; the mass ratio of the water-phase oxidant to the yellow phosphorus is (1:1)-(10:1); the reaction temperature in the water-phase oxidant is controlled at 50-85 DEG C; the reaction time is controlled between 2 hours and 4 hours; the temperature of an arsenic water phase is controlled at 100-125 DEG C to carry out boiling deoxygenation; the time is controlled at 10-30 minutes; phosphorus pentasulfide or sulfuretted hydrogen is added to the deoxidized arsenic water phase to carry out dearsenification treatment; adding phosphorus pentoxide and hydrogen peroxide to react after filtering and exposing filtrate; the dearsenified water phase is prepared into peracetic acid; the peracetic acid is recycled in a new batch of dearsenification of arsenic yellow phosphorus after the concentration is adjusted. The method has the advantages of being convenient to operate, low in production cost, environment-friendly and safe; the water-phase oxidant can be recycled.
priorityDate 2013-06-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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